HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloromethyl methyl sulfide → HCID 21286304, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloromethyl methyl sulfide | HCID 16916 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 2-(Hydroxymethyl)-1H-benzimidazole | HCID 78569 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 21286304 | HCID 21286304 | — |
Reaction Steps
Using the procedure of Preparation C1, 14.8 g of 2-hydroxymethylbenzimidazole, 4.8 g of 50% sodium hydride in oil and 8.36 ml of chloromethyl methyl sulfide in 50 ml of dimethylformamide gave 8.3 g of product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04782050 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-4a332dc46a4f41f7855d3e963d5d670b |
| Source note | uspto-grants-1988_11 |