HuagongsheHuagongshe Chemistry Print Report · For research reference only
Selenium Dioxide → 1-Methyl-1H-imidazo(4,5-c)pyridine-2-carboxaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Selenium Dioxide | HCID 24007 | — |
| Reactant | 1,2-Dimethyl-1H-imidazo[4,5-c]pyridine | HCID 4287394 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 1-Methyl-1H-imidazo(4,5-c)pyridine-2-carboxaldehyde | HCID 12239331 | 80.1% |
Reaction Steps
Using the procedure of Example 10B and starting with 357 mg of 1,2-dimethyl-1H-imidazo[4,5-c]pyridine and 270 mg of selenium dioxide in 30 ml of dioxane, there was obtained 313 mg of the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04782050 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-f16a98ce42e14e278be59bca28dae01a |
| Source note | uspto-grants-1988_11 |