HuagongsheHuagongshe Chemistry Print Report · For research reference only
Selenium Dioxide → 3-methyl-3H-imidazo[4,5-c]pyridine-2-carbaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Selenium Dioxide | HCID 24007 | — |
| Reactant | 2,3-Dimethyl-3H-imidazo[4,5-c]pyridine | HCID 12239325 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 3-methyl-3H-imidazo[4,5-c]pyridine-2-carbaldehyde | HCID 12239339 | 52.2% |
Reaction Steps
Employing the procedure of Example 10B and starting with 774 mg of 2,3-dimethyl-3H-imidazo[4,5-c]pyridine (Preparation J2) and 584 mg of selenium dioxide in 30 ml of dioxane, there was obtained 442 mg of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04782050 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-26d3138f592c4ebc824fbc6aaa24cc3a |
| Source note | uspto-grants-1988_11 |