HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → N,N-didodecylhydroxylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | HCID 19844207 | HCID 19844207 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | N,N-didodecylhydroxylamine | HCID 9864141 | 44% |
Reaction Steps
Using the general procedure of Example 2, 87.6 grams (0.2 mol) of the product of Example 5 in 800 ml of isopropanol is oxidized using 9.7 mol (0.25 mol) of 70% aqueous hydrogen peroxide solution to give 32.1 grams (44% yield) of the above-named product as a white solid melting at 85°-86° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04782105 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-0d62064e90254e8092b4f3f82faa624c |
| Source note | uspto-grants-1988_11 |