HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Allyl-4-hydroxybenzonitrile → 4-hydroxy-3-propylBenzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Allyl-4-hydroxybenzonitrile | HCID 258442 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-hydroxy-3-propylBenzonitrile | HCID 13987669 | — |
Reaction Steps
A mixture of 8.15 g of 2-allyl-4-cyanophenol prepared in Reference Example 1-(ii), 1.5 g of 5% palladium-carbon and 100 ml of methanol, was stirred in a hydrogen stream for 2.5 hours. The catalyst was removed by filtration, and the solvent was distilled off from the filtrate to obtain 7.30 g of the above identified compound as a colorless oily substance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04783462 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-b0f8e05b517f47ec9e48c258df93d05c |
| Source note | uspto-grants-1988_11 |