Veratric Acid → HCID 13364787, compound

HRID 2231870Notes

Reaction equation

HRID 2231870 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][C:11]=1[O:12][CH3:13])[C:6]([OH:8])=O.C(N1C=CN=C1)(N1C=CN=C1)=O.[NH2:26][CH2:27][C:28]1[NH:29][C:30]([CH3:33])=[CH:31][CH:32]=1>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][C:11]=1[O:12][CH3:13])[C:6]([NH:26][CH2:27][C:28]1[NH:29][C:30]([CH3:33])=[CH:31][CH:32]=1)=[O:8]

Participants

4

Reactant 3

HCID 7121Veratric AcidHCID 682631,1'-CarbonyldiimidazoleHCID 20038694HCID 20038694, compound

Product 1

HCID 13364787HCID 13364787, compound

Procedure

18.1 g (0.1 mol) of 3,4-dimethoxybenzoic acid are reacted with 17.8 g (0.11 mol) of carbonyldiimidazole and 11.0 g (0.1 mol) of 2-aminomethyl-5-methyl-pyrrole (compare Example 11), as described in Example 15.

Sources & evidence

ORD record
ord-28bdf12241d34dd680e0a5aa09d059af
Source dataset
uspto-grants-1988_11
Patent number
US04785010

Reaction notes

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