HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21284872, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1H-Imidazole-1-propanamine | HCID 78736 | — |
| Reactant | 2-(2,5-Dioxohexyl)-1H-isoindole-1,3(2H)-dione | HCID 12348451 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 21284872 | HCID 21284872 | — |
Reaction Steps
5.2 g (0.02 mol) of 6-phthalimido-2,5-hexanedione and 2.5 g (0.02 mol) of 3-(1-imidazolyl)-propylamine are stirred in 70 ml of acetic acid at 80° C. for 2 hours and the mixture is worked up as in Example 1. After ethanolic hydrochloric acid has been added, the product is filtered off and recrystallised from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04785010 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-efdaa5cb6e5b4c979265bfeeb3b3bbaf |
| Source note | uspto-grants-1988_11 |