HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 13534387, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | beta-Alanine, ethyl ester, hydrochloride | HCID 458475 | — |
| Reactant | 2-(2,5-Dioxohexyl)-1H-isoindole-1,3(2H)-dione | HCID 12348451 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 13534387 | HCID 13534387 | — |
Reaction Steps
3.9 g (0.015 mol) of 6-phthalimido-2,5-hexanedione, 3.1 g (0.02 mol) of β-alanine ethyl ester hydrochloride and 3 ml (0.02 mol) of triethylamine are stirred in 80 ml of glacial acetic acid at 50° C. for 8 hours and the mixture is worked up as in Example 27.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04785010 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-396ffea7a3a44043bac011e9a3419ec2 |
| Source note | uspto-grants-1988_11 |