HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycine methyl ester hydrochloride → HCID 13534389, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycine methyl ester hydrochloride | HCID 122755 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | 2-(2,5-Dioxoheptyl)-1H-isoindole-1,3(2H)-dione | HCID 12582894 | — |
| Solvent | Cyclohexanol | HCID 7966 | — |
| Product | HCID 13534389 | HCID 13534389 | — |
Reaction Steps
6.8 g (0.025 mol) of 7-phthalimido-3,6-heptanedione, 3.5 g (0.028 mol) of glycine methyl ester hydrochloride and 2.3 g (0.028 mol) of sodium acetate are stirred in 150 ml of cyclohexanol at 60° C. for 13 hours and the mixture is worked up as in Example 22.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04785010 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-9618e8c4a6844b0fb2c128f0d12c11ef |
| Source note | uspto-grants-1988_11 |