HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycine tert-butyl ester → HCID 13534393, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycine tert-butyl ester | HCID 151417 | — |
| Reactant | 2-(2,5-Dioxohexyl)-1H-isoindole-1,3(2H)-dione | HCID 12348451 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 13534393 | HCID 13534393 | — |
Reaction Steps
13.0 g (0.05 mol) of 6-phthalimido-2,5-hexanedione and 6.6 g (0.05 mol) of glycine tert.-butyl ester are stirred in 250 ml of tetrahydrofuran at 80° C. for 20 hours and the mixture is worked up as in Example 27.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04785010 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-dfaa8930f03a490fb32b951886f301b4 |
| Source note | uspto-grants-1988_11 |