Hydrochloric Acid → Hydrochloric Acid

HRID 2231968Notes

Reaction equation

HRID 2231968 reaction equation
[ClH:1].[CH3:2][N:3]([CH2:5][C:6]1[O:12][C:9]([CH2:10][OH:11])=[CH:8][CH:7]=1)[CH3:4]>>[ClH:1].[ClH:1].[CH3:4][N:3]([CH2:5][C:6]1[O:12][C:9]([CH2:10][OH:11])=[CH:8][CH:7]=1)[CH3:2]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 849065-((Dimethylamino)methyl)-2-furanmethanol

Product 2

HCID 313Hydrochloric AcidHCID 3086123((2-(Hydroxymethyl)-5-furyl)methyl)ammonium chloride

Procedure

In a device shown in FIG. 2, 38.5 kg/hr of aqueous 36 wt% hydrochloric acid solution was fed through a conduit 2 and 13.0 kg/hr of 5-(dimethylamino)methylfurfuryl alcohol was fed through a conduit 3 to a reactor 1 maintained at a temperature of 20° to 30° C. Aqueous hydrochloric acid solution of 5-(dimethylamino)methylfurfuryl alcohol hydrochloride thus obtained was continuously fed to a reactor 5 through a conduit 4. Under maintaining a temperature of the reactor at 50° to 60° C., 13.3 kg/hr of an aqueous 75 wt% cysteamine hydrochloride solution was continuously fed to the reactor 5 through a conduit 6. Further, a reaction product was continuously discharged from the reactor 5 through a conduit 7. Residence time at the reactor 1 was 10 minutes and the residence time at the reactor was 30 minutes.

Workup

  1. customwas fed through a conduit 3 to a reactor
  2. temperature1 maintained at a temperature of 20° to 30° C

Sources & evidence

ORD record
ord-5f12953ee4bb4ed6ac844c1c6af788b1
Source dataset
uspto-grants-1988_11
Patent number
US04785122

Reaction notes

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