HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2-Triphenylmethylamino-4-thiazolyl)glyoxylic acid → HCID 13578647, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2-Triphenylmethylamino-4-thiazolyl)glyoxylic acid | HCID 11133448 | — |
| Reactant | (2-Tritylaminothiazol-4-yl)methoxyamine | HCID 21285079 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 13578647 | HCID 13578647 | 87% |
Reaction Steps
3.1 g of 2-(2-tritylaminothiazol-4-yl)glyoxalic acid was dissolved in 170 ml of methanol, 2.9 g of the (2-tritylaminothiazol-4-yl)methoxyamine was added thereto, and stirred at room temperature for 4 hours. The formed precipitates were filtered off and washed with 20 ml of methanol to obtain 5.1 g of (Z)-2-(2-tritylaminothiazol-4-yl)-2-[(2-tritylaminothiazol-4-yl)methoxyimino]acetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04785090 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-f5c6761cf1224a8fb2160dcd74b89c4c |
| Source note | uspto-grants-1988_11 |