HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Pyridinecarboxaldehyde → HCID 137192606, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Pyridinecarboxaldehyde | HCID 13389 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 137192606 | HCID 137192606 | 73.1% |
Reaction Steps
A solution of 4-pyridine carboxaldehyde (25.0 g, 233 mmol) in 100 ml of methanol was treated with hydroxylamine hydrochloride (17.84 g, 250 mmol) and stirred 15 minutes at room temperature. The resulting white solid was collected by filtration and dried in vacuo to provide 27.0 g of 4-pyridine carboxaldehyde oxime, hydrochloride, mp 246°-247° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04786648 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-bd302f57bbee401283b20fd4682b4074 |
| Source note | uspto-grants-1988_11 |