HuagongsheHuagongshe Chemistry Print Report · For research reference only
(E)-4-(4-isoquinolinyl)-3-buten-1-amine → 4-Isoquinolinebutanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (E)-4-(4-isoquinolinyl)-3-buten-1-amine | HCID 14750834 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-Isoquinolinebutanamine | HCID 14994126 | 88.4% |
Reaction Steps
A solution of 1 g of (E)-4-(4-isoquinolinyl)-3-buten-1-amine in 20 mL of ethanol was hydrogenated over 0.12 g of 10% Pd/C at room temperature and atmospheric pressure. After 8 hours, the catalyst was removed by filtration and the filtrate was concentrated to yield 0.893 g of 4-isoquinolinebutanamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04786646 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-61506bc2486d485e9a93464b032aea6c |
| Source note | uspto-grants-1988_11 |