HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylene Oxide → HCID 86742540, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylene Oxide | HCID 6354 | — |
| Reactant | HCID 14324234 | HCID 14324234 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86742540 | HCID 86742540 | 97% |
Reaction Steps
Next 355 parts of 2,5-dimethyl-8-methoxytetrahydroquinoline in 0.4 l ethanol with 86 parts ethylene oxide was reacted under pressure at 175° C. for 10 hours. The solvent was stripped under reduced pressure to an oil which eventually solidifed to give 97% N-(β-hydroxyethyl)-2,5-dimethyl-8-methoxytetrahydroquinoline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04788121 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-467d069ab3494aa29c30634c1a77ac7a |
| Source note | uspto-grants-1988_11 |