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HRID2232231

反应详情

EQUATION

反应方程式

HRID 2232231 的结构方程式

REACTANTS

反应物

2
结构：CNCC(C)O
HCID86049

1-(Methylamino)propan-2-ol

C4H11NO

结构：Clc1ccc2c(c1)c(-c1ccccc1)nn1c(Cl)nnc21
HCID21283345

未命名化合物

PRODUCTS

生成物

1
结构：CC(O)CN(C)c1nnc2c3ccc(Cl)cc3c(-c3ccccc3)nn12
HCID3071243

1-[(8-Chloro-6-phenyl[1,2,4]triazolo[3,4-a]phthalazin-3-yl)(methyl)amino]propan-2-ol

C19H18ClN5O

收率 73%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO.ClC(Cl)Cl
溶剂HCID21889567

未命名化合物

PROCEDURE

实验过程

The compound of the title is prepared by following substantially the same procedure outlined in example 122 but starting from 3,8-dichloro-6-phenyl-1,2,4-triazolo[3,4-a]phthalazine and (2-hydroxypropyl)methylamine. Yield: 73%. M.p. 236°-38° C. (from ethanol/chloroform).

WORKUP

后处理

  1. customThe compound of the title is prepared