HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(Methylamino)propan-2-ol → 2-Propanol, 1-((8-chloro-6-phenyl-1,2,4-triazolo(3,4-a)phthalazin-3-yl)methylamino)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(Methylamino)propan-2-ol | HCID 86049 | — |
| Reactant | 3,8-Dichloro-6-phenyl-1,2,4-triazolo[3,4-a]phthalazine | HCID 21283345 | — |
| Solvent | Chloroform ethanol | HCID 21889567 | — |
| Product | 2-Propanol, 1-((8-chloro-6-phenyl-1,2,4-triazolo(3,4-a)phthalazin-3-yl)methylamino)- | HCID 3071243 | 73% |
Reaction Steps
The compound of the title is prepared by following substantially the same procedure outlined in example 122 but starting from 3,8-dichloro-6-phenyl-1,2,4-triazolo[3,4-a]phthalazine and (2-hydroxypropyl)methylamine. Yield: 73%. M.p. 236°-38° C. (from ethanol/chloroform).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04788186 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-0c34e8df8dbc4792a9e5937827f11030 |
| Source note | uspto-grants-1988_11 |