p-Fluoronitrobenzene → HCID 70418345, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of the product of (i) above (7.76 g), 4-fluoronitrobenzene (5.50 g) and sodium carbonate (4.50 g) in N,N-dimethylformamide (40 ml) was heated at 100° C. with stirring for 4 hours. The mixture was evaporated to about half volume and filtered. The residue was washed with ethanol followed by warm water and then dried to give the title compound (9.41 g), m.p. 230°-232° C.

Provenance & Evidence