HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 88500541, compound → HCID 88500301, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 88500541 | HCID 88500541 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 88500301 | HCID 88500301 | — |
Reaction Steps
Two grams of 7β-[2-(2-amino-5-chlorothiazol-4-yl)-2(Z)-(tert-butoxycarbonylmethoxyimino)acetamido]-3-(3-oxobutyryloxymethyl)-3-cephem-4-carboxylic acid is dissolved in 20 ml of trifluoroacetic acid. The solution is stirred at room temperature for 1 hour and then evaporated to dryness under reduced pressure to give crude 7β-[2-(2-amino-5-chlorothiazol-4-yl)-2(Z)-(carboxymethoxyimino)acetamido]-3-(3-oxobutyryloxymethyl)-3-cephem-4-carboxylic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04788185 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-dfbed8bb47c346e0b2b736114878c7f1 |
| Source note | uspto-grants-1988_11 |