HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 13769195, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 21283588 | HCID 21283588 | — |
| Reactant | Cyclohexane ethylacetate | HCID 21867204 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 13769195 | HCID 13769195 | — |
Reaction Steps
The procedure is as in Example 44, but starting with 3-[(2-phenyl-4-quinolyl)oxy]propanic acid (1.25 g), thionyl chloride (1.25 cc) in chloroform (100 cc) and diethylamine (2.66 cc). After chromatography of the residue on silica gel using the eluant cyclohexane/ethyl acetate (50:50 by volume), N,N-diethyl-3-[(2-phenyl-4-quinolyl)oxy]propanamide (0.43 g), m.p. 94° C., is isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04788204 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-59239f284ad94e3ab9dcf2804b21f3e8 |
| Source note | uspto-grants-1988_11 |