HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Acrylate → beta-Hydroxy-alpha-methylenebenzeneheptanoic acid methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Reactant | Dabco | HCID 9237 | — |
| Reactant | Benzenepentanal | HCID 561886 | — |
| Product | beta-Hydroxy-alpha-methylenebenzeneheptanoic acid methyl ester | HCID 14348901 | — |
Reaction Steps
A mixture of 8.4 g (52 mmol) of 5-phenylpentanal, 8.95 g (104 mmol) of methyl acrylate and 200 mg of 1,4-diazabicyclo[2.2.2]octane is allowed to stand at room temperature for 120 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04788306 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-28e14a4b6f5943cabbed693ec45faa3d |
| Source note | uspto-grants-1988_11 |