HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexyl isocyanate → HCID 20523351, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexyl isocyanate | HCID 18502 | — |
| Reactant | 3-(Dimethylamino)-1-propanol | HCID 76646 | — |
| Product | HCID 20523351 | HCID 20523351 | — |
Reaction Steps
77.3 g of 3-dimethylamino-1-propanol are reacted with 94 g of cyclohexyl isocyanate in accordance with Example 13. Distillation of the reaction product yields 153.4 g (92.8%) of analytically pure product (analysis by gas chromatography) with a boiling point of 105° C./0.015 torr. IR spectrum: 3320 cm-1NH, 1700 cm-1C=O, no bands between 2000 and 2500 cm-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04352913 |
| Source dataset | uspto-grants-1982_10 |
| ORD ID | ord-da6e18ca016b446db386443344080076 |
| Source note | uspto-grants-1982_10 |