1-Iodopropane → HCID 22345157, compound

HRID 2232901Notes

Reaction equation

HRID 2232901 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]([F:11])([F:10])[F:9])=[CH:4][C:3]=1[N:12]1[CH2:17][CH2:16][NH:15][CH2:14][CH2:13]1.I[CH2:19][CH2:20][CH3:21]>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]([F:9])([F:10])[F:11])=[CH:4][C:3]=1[N:12]1[CH2:17][CH2:16][N:15]([CH2:19][CH2:20][CH3:21])[CH2:14][CH2:13]1

Participants

3

Reactant 2

HCID 336431-IodopropaneHCID 3830901HCID 3830901, compound

Product 1

HCID 22345157HCID 22345157, compound

Procedure

Beginning with 1-(2-Chloro-5-trifluoromethyl-phenyl)-piperazine and 1-iodopropane, the title compound was recovered by the procedure described in Example 2. m.p. 234° C. (HCl), MS m/z (rel. intensity, 70 eV) 306 (M+, 20), 279 (34), 277 (bp), 70 (99), 56 (48).

Workup

  1. customthe title compound was recovered by the procedure

Sources & evidence

ORD record
ord-b866565e36fc493a9fe28e1d0068035e
Source dataset
uspto-grants-2010_05
Patent number
USRE041315E1

Reaction notes

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