Butyl bromide → 1-Butyl-4-(4-Methyl-3-nitro-phenyl)-piperazine

HRID 2232907Notes

Reaction equation

HRID 2232907 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH2:13][CH2:12][NH:11][CH2:10][CH2:9]2)=[CH:4][C:3]=1[N+:14]([O-:16])=[O:15].[CH2:17](Br)[CH2:18][CH2:19][CH3:20]>>[CH2:17]([N:11]1[CH2:10][CH2:9][N:8]([C:5]2[CH:6]=[CH:7][C:2]([CH3:1])=[C:3]([N+:14]([O-:16])=[O:15])[CH:4]=2)[CH2:13][CH2:12]1)[CH2:18][CH2:19][CH3:20]

Participants

3

Reactant 2

HCID 8002Butyl bromideHCID 47388041-(4-Methyl-3-nitrophenyl)piperazine

Product 1

HCID 223451931-Butyl-4-(4-Methyl-3-nitro-phenyl)-piperazine

Procedure

Beginning with 1-(4-methyl-3-nitro-phenyl)-piperazine and 1-butylbromide, the title compound was recovered by the procedure described in Example 2. MS m/z (rel. intensity, 70 eV) 277 (M+, 23), 234 (bp), 191 (17), 70 (64), 56 (33).

Workup

  1. customthe title compound was recovered by the procedure

Sources & evidence

ORD record
ord-9c4fa440255f478393dff275808ae001
Source dataset
uspto-grants-2010_05
Patent number
USRE041315E1

Reaction notes

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