Iodoethane → HCID 22345179, compound

HRID 2232911Notes

Reaction equation

[F:1][C:2]1[CH:3]=[C:4]([N:12]2[CH2:17][CH2:16][NH:15][CH2:14][CH2:13]2)[CH:5]=[C:6]([C:8]([F:11])([F:10])[F:9])[CH:7]=1.I[CH2:19][CH3:20]>>[CH2:19]([N:15]1[CH2:16][CH2:17][N:12]([C:4]2[CH:5]=[C:6]([C:8]([F:10])([F:11])[F:9])[CH:7]=[C:2]([F:1])[CH:3]=2)[CH2:13][CH2:14]1)[CH3:20]

Participants

Reactant 2

HCID 6340Iodoethane

HCID 11357080HCID 11357080, compound

Product 1

HCID 22345179HCID 22345179, compound

Procedure

Beginning with 1-(3-fluoro-5-trifluoromethyl-phenyl)-piperazine and 1-iodoethane, the title compound was recovered by the procedure described in Example 2; MS m/z (rel. intensity, 70 eV) 276 (M+, 46), 261 (41), 190 (30), 84 (30), 57 (bp).

Workup

customthe title compound was recovered by the procedure

Sources & evidence

ORD record: ord-7654ea98c2cb4582911cc2fabe2353cd
Source dataset: uspto-grants-2010_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: USRE041315E1

Reaction notes

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