2-Bromopropane → HCID 22345185, compound
Reaction equation
[F:1][C:2]1[CH:3]=[C:4]([N:12]2[CH2:17][CH2:16][NH:15][CH2:14][CH2:13]2)[CH:5]=[C:6]([C:8]([F:11])([F:10])[F:9])[CH:7]=1.[CH:18](Br)([CH3:20])[CH3:19]>>[CH:18]([N:15]1[CH2:16][CH2:17][N:12]([C:4]2[CH:5]=[C:6]([C:8]([F:10])([F:11])[F:9])[CH:7]=[C:2]([F:1])[CH:3]=2)[CH2:13][CH2:14]1)([CH3:20])[CH3:19]Participants
3
Procedure
Beginning with 1-(3-fluoro-5-trifluoromethyl-phenyl)-piperazine and isopropylbromide, the title compound was recovered by the procedure described in Example 2; MS m/z (rel. intensity, 70 eV) 290 (M+, 30), 275 (bp), 190 (20), 84 (23), 56 (64).
Workup
- customthe title compound was recovered by the procedure
Sources & evidence
- ORD record
- ord-a4c620355855424b83256a06eb9486da
- Source dataset
- uspto-grants-2010_05
- Patent number
- USRE041315E1
Reaction notes
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