1-Iodopropane → HCID 22345169, compound

HRID 2232914Notes

Reaction equation

HRID 2232914 reaction equation
[CH3:1][S:2]([C:5]1[CH:6]=[C:7]([N:13]2[CH2:18][CH2:17][NH:16][CH2:15][CH2:14]2)[CH:8]=[CH:9][C:10]=1[O:11][CH3:12])(=[O:4])=[O:3].[CH2:19](I)[CH2:20][CH3:21]>>[CH3:1][S:2]([C:5]1[CH:6]=[C:7]([N:13]2[CH2:14][CH2:15][N:16]([CH2:19][CH2:20][CH3:21])[CH2:17][CH2:18]2)[CH:8]=[CH:9][C:10]=1[O:11][CH3:12])(=[O:3])=[O:4]

Participants

3

Reactant 2

HCID 336431-IodopropaneHCID 22345160HCID 22345160, compound

Product 1

HCID 22345169HCID 22345169, compound

Procedure

Beginning with 1-(3-Methanesulfonyl-4-methoxy-phenyl)-piperazine and n-Pr-I, the title compound was recovered by the procedure described in Example 2;: MS m/z (rel. intensity, 70 eV)) 312 (M+, 38), 284 (17), 283 (bp), 70 (49), 56 (17).

Workup

  1. customthe title compound was recovered by the procedure

Sources & evidence

ORD record
ord-e18e0f1cc42642268572f450cbcf6a45
Source dataset
uspto-grants-2010_05
Patent number
USRE041315E1

Reaction notes

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