Piperazine → HCID 22345190, compound

HRID 2232938Notes

Reaction equation

Br[C:2]1[CH:3]=[CH:4][C:5]([Cl:12])=[C:6]([S:8]([CH3:11])(=[O:10])=[O:9])[CH:7]=1.[NH:13]1[CH2:18][CH2:17][NH:16][CH2:15][CH2:14]1>>[Cl:12][C:5]1[CH:4]=[CH:3][C:2]([N:13]2[CH2:18][CH2:17][NH:16][CH2:15][CH2:14]2)=[CH:7][C:6]=1[S:8]([CH3:11])(=[O:10])=[O:9]

Participants

Reactant 2

HCID 4837Piperazine

HCID 22345199346729-65-5

Product 1

HCID 22345190HCID 22345190, compound

Procedure

Beginning with 5-bromo-2-chloro-methanesulfonyl-benzene and piperazine, the title compound was recovered by the procedure described in Example 1. MS m/z (rel. intensity, 70 eV)) 274 (M+, 20), 234 (40), 232 (bp), 153 (9), 56 (12).

Workup

customthe title compound was recovered by the procedure

Sources & evidence

ORD record: ord-c0d67ae504ee45ada20edc0cf0df026e
Source dataset: uspto-grants-2010_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: USRE041315E1

Reaction notes

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