HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → HCID 68678087, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | HCID 68676527 | HCID 68676527 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 68678087 | HCID 68678087 | — |
Reaction Steps
A solution of 0.50 g of the product of Step F and 0.40 g of ethanolamine in THF (6 mL) was heated at reflux for 16 h. After cooling the reaction mixture to ambient temperature, solvents were removed and the residue was purified by silica gel chromatography to yield the title compound as a white solid. MS (M+H+)=252.3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07709473B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-543f1bd9aebb4f73add199eacbf683b5 |
| Source note | uspto-grants-2010_05 |