HCID 68677268, compound → HCID 68675893, compound

Participants

Reaction Steps

A solution of 20 mg of 1-(8-isopropylamino-3-oxo-2,3-dihydro-[1,2,4]triazolo[4,3-a]pyrazin-6-yl)-cyclopentanecarboxylic acid in AcOH (3.0 mL) was warmed to 120° C. for 30 min. The reaction was cooled to ambient temperature and diluted with water. The mixture was extracted with EtOAc, the organic layer was washed with water (2×), dried over magnesium sulfate, filtered, and concentrated to leave the title compound as a tan solid. MS (M+H+)=262.3.

Provenance & Evidence