Isopropylamine → HCID 68676396, compound

Participants

Reaction Steps

A solution of 29 mg of the product of Step A and 118 mg of isopropylamine in THF (5.0 mL) was heated at reflux for 16 h. The reaction was concentrated to one-quarter volume, diluted with water, and the pH was adjusted to pH 2 with 2N HCl. The solid was collected and triturated for one h in isopropyl ether at 60° C. before being collected and dried to give the title compound as a tan solid. MS (M+H+)=270.1.

Provenance & Evidence