HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 68677253, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | 2-(Pyridin-3-yl)ethan-1-amine | HCID 854051 | — |
| Reactant | HCID 68676862 | HCID 68676862 | — |
| Product | HCID 68677253 | HCID 68677253 | — |
Reaction Steps
A solution of 31 mg of the product of Step A and 120 mg of 2-pyridin-3-yl-ethylamine in THF (3.0 mL) was heated at reflux for 16 h. The solvent was removed and the residue was purified by silica gel chromatography to afford the title compound as a light yellow solid. MS (M+H+)=403.4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07709473B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-72c727a5dae4493abd2c41a9e5af5520 |
| Source note | uspto-grants-2010_05 |