HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68676710, compound → HCID 68677961, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68676710 | HCID 68676710 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68677961 | HCID 68677961 | — |
Reaction Steps
A solution of 30 mg of 6-isopropyl-8-isopropylamino-5-(3-methyl-but-1-enyl)-2H-[1,2,4]triazolo[4,3-a]pyrazin-3-one in EtOH (10 mL) was treated with 50 mg of 10% Pd/C. The mixture was hydrogenated at 35 psi for one h and the solids were removed by filtration through diatomaceous earth. The filtrate was concentrated to provide the title compound as a white solid. MS (M+H+)=304.4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07709473B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-2f95526bce4d470eb61c7076bdcd2d3b |
| Source note | uspto-grants-2010_05 |