3,4-Dichloroaniline → 2-(3,4-Dichlorophenylamino)-4-thiocyanato-5-nitro-pyrimidine

Participants

Reaction Steps

2.47 g of 3,4-dichloroaniline in 12 ml ethanol are added to 3.00 g of 2-chloro-4-thiocyanato-5-nitro-pyrimidine in 40 ml toluene at ambient temperature. The mixture is stirred for another 16 hours, the solid is suction filtered, washed twice with 30 ml toluene and then once with 30 ml of ethanol and dried.

Provenance & Evidence