HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68448107, compound → HCID 86623073, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68448107 | HCID 68448107 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86623073 | HCID 86623073 | 81% |
Reaction Steps
A solution of 1,1-dimethylethyl 7-(hydroxymethyl)-2,3-dihydro-1H-pyrido[3,4-b][1,4]oxazine-1-carboxylate (0.78 g, 2.9 mmol) in dichloromethane (100 ml) was treated with manganese(IV) oxide (2.02 g, 23.3 mmol) and stirred overnight. Filtration and evaporation afforded a white solid (0.62 g, 81%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07709483B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-81f98bd569134c77ae1bf8a85f7b5306 |
| Source note | uspto-grants-2010_05 |