HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59295378, compound → HCID 59295412, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59295378 | HCID 59295378 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 59295412 | HCID 59295412 | 88% |
Reaction Steps
5.30 g 2-Cyclohex-1-enyl-4-methoxymethyl-oxazole-5-carboxylic acid methyl ester were dissolved in 40 ml methanol. 500 mg palladium on charcoal (10%) were added and the reaction mixture was stirred under an atmosphere of hydrogen overnight. The catalyst was filtered off through a pad of celite, the filtrate was evaporated in vacuo to obtain 4.70 g 2-Cyclohexyl-4-methoxymethyl-oxazole-5-carboxylic acid methyl ester as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07709481B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-44f9874247104dd3938c755b4a13274e |
| Source note | uspto-grants-2010_05 |