HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59295396, compound → HCID 59295435, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59295396 | HCID 59295396 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 59295435 | HCID 59295435 | 97.7% |
Reaction Steps
580 mg 2-Cyclohex-1-enyl-4-morpholin-4-ylmethyl-oxazole-5-carboxylic acid ethyl ester were dissolved in 15 ml methanol. 50 mg palladium on charcoal (10%) were added and the reaction mixture was stirred under an atmosphere of hydrogen for one hour. The catalyst was filtered off through a pad of celite, the filtrate was evaporated in vacuo to obtain 570 mg 2-Cyclohexyl-4-morpholin-4-ylmethyl-oxazole-5-carboxylic acid ethyl ester as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07709481B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-0175df0891b743339109ba8937a36c74 |
| Source note | uspto-grants-2010_05 |