HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 58730647, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 58730638 | HCID 58730638 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 58730647 | HCID 58730647 | — |
Reaction Steps
Starting from 450 mg (0.80 mmol) of the ester from Example 21A, reaction in analogy to general method [E] with 96 mg (2.40 mmol) of sodium hydroxide in 21.5 ml of dioxane results in 407.5 mg (93% of theory) of the target compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07709491B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-f93d427a9f814d088dd2ae7d06498c82 |
| Source note | uspto-grants-2010_05 |