HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 136399784, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 131728104 | HCID 131728104 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 136399784 | HCID 136399784 | 92% |
Reaction Steps
A solution of (16) (0.30 g, 1.32 mmol) in 10% sodium hydroxide (5 ml) and ethanol (5 ml) was heated under reflux for 1.5 h. When cooled to room temperature the ethanol was removed in vacuo and the mixture was filtered to give (18) as a white solid (0.20 g, 92%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07709514B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-d803c5a68ce14826894f0ad760e7ac3f |
| Source note | uspto-grants-2010_05 |