HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 86609239, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 86609238 | HCID 86609238 | — |
| Catalyst | Platinum | HCID 23939 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 86609239 | HCID 86609239 | — |
Reaction Steps
The product from step (iii) (1.0 g) was dissolved in EtOAc (20 ml), triethylamine (1.1 ml) added, followed by 5% Pt/C (50 mg) and hydrogenated at 1 atm and RT for 6 h. The catalyst was filtered off and the filtrate evaporated to give a light brown solid. Yield 800 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07709521B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-127cb798290d47ef8bf1eff458003817 |
| Source note | uspto-grants-2010_05 |