2,2-Dimethyl-1,3-dioxane-4,6-dione → Ethyl 4-methoxy-3-oxobutanoate

HRID 2233807Notes

Reaction equation

C[C:2]1([CH3:10])[O:7][C:6](=[O:8])[CH2:5][C:4](=[O:9])O1.[CH3:11][O:12][CH2:13]C(Cl)=O>>[CH3:11][O:12][CH2:13][C:4](=[O:9])[CH2:5][C:6]([O:7][CH2:2][CH3:10])=[O:8]

Participants

Reactant 2

HCID 162492,2-Dimethyl-1,3-dioxane-4,6-dione

HCID 96623Methoxyacetyl chloride

Product 1

HCID 12645099Ethyl 4-methoxy-3-oxobutanoate

Procedure

The title compound was prepared in a manner analogous to Intermediate 123 starting from 2,2-dimethyl-1,3-dioxane-4,6-dione and methoxyacetyl chloride.

Sources & evidence

ORD record: ord-3876cc7d748441bea038073af47cc70f
Source dataset: uspto-grants-2010_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07709503B2

Reaction notes

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