HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 178497950, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | Methyl 6-aminopyridine-2-carboxylate | HCID 13809143 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 178497950 | HCID 178497950 | 87% |
Reaction Steps
Methyl 6-aminopyridine-2-carboxylate (Intermediate 121, 3.3 g, 22 mmol) was dissolved in acetone and to this was added a solution of mCPBA (5.9 g, 23.5 mmol) in acetone. After stirring overnight, the acetone was removed and the residue was suspended in 3 N HCl. The precipitate was filtered off to give the HCl salt (3.57 g, 87%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07709503B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-c5dbe31a31994390a66400b84812d3f9 |
| Source note | uspto-grants-2010_05 |