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HRID2233899

反应详情

EQUATION

反应方程式

HRID 2233899 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)c1cc(Cl)c2ccccc2n1
HCID19066063

未命名化合物

结构：COC(=O)c1cnc(N2CCC(NC(=O)OC(C)(C)C)CC2)s1
HCID59679281

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)c1cc(N2CCC(NC(=O)OC(C)(C)C)CC2)c2ccccc2n1
HCID46941938

未命名化合物

PROCEDURE

实验过程

The title compound was prepared by a procedure analogous to Intermediate 133 starting with methyl 4-chloroquinoline-2-carboxylate (WO 9505378). The product was purified on a silica gel flash column (0→5% MeOH in DCM) followed by recrystallization from EtOAc.

WORKUP

后处理

  1. customThe product was purified on a silica gel flash column (0→5% MeOH in DCM)
  2. customfollowed by recrystallization from EtOAc