O-Methylhydroxylamine hydrochloride → HCID 86761103, compound

HRID 2233982Notes

Reaction equation

HRID 2233982 reaction equation
[Cl:1][C:2]1[C:6]([Cl:7])=[C:5]([CH3:8])[NH:4][C:3]=1[C:9]([NH:11][CH:12]1[CH2:17][CH2:16][N:15]([C:18]2[CH:19]=[C:20]([C:25](O)=[O:26])[NH:21][C:22](=[O:24])[N:23]=2)[CH2:14][CH2:13]1)=[O:10].Cl.[O:29]([NH2:31])[CH3:30]>>[Cl:1][C:2]1[C:6]([Cl:7])=[C:5]([CH3:8])[NH:4][C:3]=1[C:9]([NH:11][CH:12]1[CH2:17][CH2:16][N:15]([C:18]2[CH:19]=[C:20]([C:25]([NH:31][O:29][CH3:30])=[O:26])[NH:21][C:22](=[O:24])[N:23]=2)[CH2:14][CH2:13]1)=[O:10]

Participants

3

Reactant 2

HCID 521874O-Methylhydroxylamine hydrochlorideHCID 68579898HCID 68579898, compound

Product 1

HCID 86761103HCID 86761103, compound

Procedure

The title compound was synthesized by an analogous method to Example 8 starting from 6-(4-{[(3,4-dichloro-5-methyl-1H-pyrrol-2-yl)carbonyl]amino}piperidin-1-yl)-2-oxo-2,3-dihydropyrimidine-4-carboxylic acid (Example 173) and methoxylamine hydrochloride.

Sources & evidence

ORD record
ord-16f8f5e9b53a41c59dca331f6a7b12d5
Source dataset
uspto-grants-2010_05
Patent number
US07709503B2

Reaction notes

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