HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromoisoxazole-5-carboxylic acid → HCID 68582525, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromoisoxazole-5-carboxylic acid | HCID 327716 | — |
| Reactant | HCID 68579996 | HCID 68579996 | — |
| Product | HCID 68582525 | HCID 68582525 | 33.6% |
Reaction Steps
The title compound was prepared via the procedure described in Example 1 from 182 mg (0.5 mmol) of 3,4-dichloro-5-methyl-N-piperidin-4-yl-1H-pyrrole-2-carboxamide hydrochloride (Intermediate 1) and 103 mg (0.54 mmol) of 3-bromoisoxazole-5-carboxylic acid (Intermediate 120), to afford the title compound as a white solid, (65 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07709503B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-c69f57e06ff64c1ea2980921d7ec3433 |
| Source note | uspto-grants-2010_05 |