Phenacyl bromide → HCID 22462654, compound

Participants

Reaction Steps

A reaction vessel was charged with 10.1 g of triethylamine, 19.9 g of phenacylbromide and 200 g of methanol, and they were stirred at room temperature for 6 hours. By evaporating methanol from this solution, 29.9 g of a white crystalline matter were obtained. This was washed with diethyl ether, then dried under reduced pressure, to obtain 24.9 g of an intermediate triethylphenacyl ammonium bromide (yield: 83%).

Provenance & Evidence