Benzaldehyde → HCID 68581073, compound

HRID 2234259Notes

Reaction equation

HRID 2234259 reaction equation
[C:1]([O:5][C:6](=[O:20])[NH:7][CH:8]1[CH2:17][C:16]2[C:11](=[CH:12][CH:13]=[C:14]([C:18]#[N:19])[CH:15]=2)[NH:10][CH2:9]1)([CH3:4])([CH3:3])C.[CH:21](=O)[C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1>>[OH:5][CH:1]1[CH2:4][CH2:3][CH:1]([O:5][C:6](=[O:20])[NH:7][CH:8]2[CH2:17][C:16]3[C:11](=[CH:12][CH:13]=[C:14]([C:18]#[N:19])[CH:15]=3)[N:10]([CH2:21][C:22]3[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=3)[CH2:9]2)[CH2:4][CH2:3]1

Participants

3

Reactant 2

HCID 240BenzaldehydeHCID 66692977tert-Butyl (6-cyano-1,2,3,4-tetrahydroquinolin-3-yl)carbamate

Product 1

HCID 68581073HCID 68581073, compound

Procedure

The title compound was prepared from (6-cyano-1,2,3,4-tetrahydroquinolin-3-yl)-carbamic acid tert-butyl ester, prepared as described in Example 1C, and benzaldehyde by procedures analogous to those described in Example 3A and 31.

Workup

  1. customprepared

Sources & evidence

ORD record
ord-0adbf0386d5a41c5a9f1269b9cdbc238
Source dataset
uspto-grants-2010_05
Patent number
US07709647B2

Reaction notes

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