HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 54339371, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-Chloropropionyl chloride | HCID 69364 | — |
| Reactant | 5-Amino-2,4-dichloropyrimidine | HCID 257797 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 54339371 | HCID 54339371 | — |
Reaction Steps
To a solution of 5-Amino-2,4-dichloropyrimidine (Chempacific; 100 mg, 0.610 mmol) in THF (2 mL) was added triethylamine (170 μL, 1.22 mmol) followed by 3-Chloropropionyl Chloride (Aldrich; 64 mL, 0.671 mmol) The reaction was stirred at room temperature for 18 hrs.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07709471B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-6aa11810028e4c4294750143955e2a36 |
| Source note | uspto-grants-2010_05 |