HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2-Dimethyaminoethylamine → 4-amino-3-chloro-N-(2-dimethylaminoethyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2-Dimethyaminoethylamine | HCID 57163524 | — |
| Reactant | 4-amino-3-chloro-N-(1-ethyl-4-piperidyl)benzamide | HCID 64321494 | — |
| Product | 4-amino-3-chloro-N-(2-dimethylaminoethyl)benzamide | HCID 59763680 | — |
Reaction Steps
The title compound was prepared by an analogous method to the preparation of Intermediate 212, on a 15 mmol scale utilising 2,2-Dimethyaminoethylamine (Aldrich; 1.455 g, 16.5 mmol), as a white solid (1.45 g, 40%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07709471B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-97198d5f9595424fa0a4eb94b422e518 |
| Source note | uspto-grants-2010_05 |