HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → tert-butyl N-(4-pyrrolidin-1-ylcyclohexyl)carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | tert-butyl N-[4-(azetidin-1-yl)cyclohexyl]carbamate | HCID 68684591 | — |
| Product | tert-butyl N-(4-pyrrolidin-1-ylcyclohexyl)carbamate | HCID 21882609 | — |
Reaction Steps
The title compound was prepared by an analogous method to the preparation of Intermediate 227, on a 2.34 mmol scale utilising pyrrolidine (Aldrich; 250 μL, 3.04 mmol), as a white solid (175 mg, 44%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07709471B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-e608af0bf27c42a48f8f6bbb403948c9 |
| Source note | uspto-grants-2010_05 |